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Wet Granulation: End-Point Determination and Scale-Up
- Introduction
- What Is An End-Point?
- What can Be Measured on a Mixer-Granulator?
- Current
- Voltage
- Capacitance
- Conductivity
- Probe Vibration
- Boots Diosna Probe
- Chopper Speed
- Impeller or Motor Shaft Speed
- Motor Slip and Motor Load Analyzer
- Impeller Tip Speed
- Relative Swept Volume
- Temperature
- Binder Addition Rate
- Power Consumption
- Impeller Torque
- Torque Rheometer
- Reaction Torque
- Other Possibilities
- Emerging Technology
- End-Point Determination
- End-Point Scale-Up
- Scale-Up Attempts
- Dimensional Analysis
- Principle of Similitude
- Dimensionless Numbers
- Comparison of Attainable Froude Numbers
- Π-theorem (Buckingham)
- Scientific Scale-Up Procedure
- Relevance List
- Dimensional Matrix
- Case Study I: Leuenberger (1979,1983)
- Case Study II: Landin et al. (1996)
- Case Study III: Faure et al. (1998)
- Case Study IV: Landin et al. (1999)
- Case Study V: Faure et al. (1999)
- Case Study VI: Hutin et al. (2004)
- Practical Considerations for End-Point Determination and Scale-Up
- References
- Appendix
- Articles of Further Interest
Abstract
Wet granulation is used mainly to improve flow and compressibility of powders, and to prevent segregation of the blend components. Particle size of the granulate is affected by the quantity and feeding rate of the granulating liquid.
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